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Issue # 72 - November/December 1981

Now you can use a "secret" industrial technique to produce your own fuel alcohol!

Mother's Home-Scale Vacuum Distillery

Over the past several years, as many of you already know, there's been a tremendous amount of public interest in homeproduced fuel alcohol, especially among people in the agricultural community. Unfortunately, a small—scale operation—such as that which might be set up by a handy individual with a limited budgetoften isn't as time—and energy—efficient as are commercial plants . . . simply because a backyard facility likely doesn't have the twin advantages of large capacity and state-of-the-art engineering.

As a result, the owner of an "appropriate"—sized fuel factory—though enjoying the satisfactions of lower initial plant cost and energy independence—might still have to "pay the piper" in terms of operating convenience and production expense. So, in an attempt to combine the desirable features of a homestead backyard still and an industrial behemoth, MOTHER's researcher Clarence Goosen has spent the better part of a year designing and building a distillation system that operates under vacuum . . . to deliver a contin uous flow of 185 proof ethanol at the lowest possible operating expense.

CONVENTIONAL CONSTRUCTION

A sight glass allows a visual check on ethanol leaving the condenser The vacuum pump and motor assembly.
A three-way valve controls reflux temperatures.
Our continuous proofing device.
The mash discharge pump.

In essence, the cost-conscious designerdeveloped an efficient atmosphere still, which he then modified to incorporate a vacuum system. Thus the unit's "negative pressure" capability is an option that can bechosen or discarded by the builder.

Clarence's still uses [1] a reboilerheated by MOTHER's multifuel hot-oil furnace (see issue 65, page 126)—to serve as the "steaming vat" from which vapors rise, [2] a stripper column, filled with polypropylene pall rings, to remove the alcohol from the mash, [3] a rectifier column, also pall-ring packed, which further fractionates (that is, upgrades to a higher proof)the rising vapors, [4] a refluxing section (this assembly includes an internal heat exchanger and a high-proof-alcohol feed line) to keep the upper part of the rectifierat a constant temperature below that found in the lower section of the tube, and to provide a source of high-grade condensed ethanol that serves to enrich and thus strengthen—the ascending vapors, and [5] a two-stage condenser column, which uses incoming mash and cold water, respectively, to remove the final product first from the driven vapor and then from the discharge air (that which is drawn through the vacuum pump). You'll notice, too, that the relatively compact design utilizes an interconnecting pipepositioned between the stripper and the rectifier column—in order to halve the total height of the tower . . . which would otherwise be over 30 feet tall!

HOW IT WORKS

In operation, MOTHER's newest distillery has proved to be quite effective, thanks to a combination of the vacuum system and several other desirable energy- and timesaving features. Briefly, here's how it works: Heat is constantly being added to the reboiler via an internal tubing network filled with hot oil. Because this chamberalong with all the other "sealed" components in the still-is under a vacuum of approximately 22 inches of mercury, the mash within the container will boil at only 125F (this, of course, is due to the fact that the liquid requires less heat to come to a "roll" under a negative pressure condition).

As the liquid boils, it gives off an alcohol-andwater vapor, which is driven up the stripper column where it loses its heat to fresh mash coming down the tube. This arrangement—it simply amounts to using mash rather than water as coolant in selected condensers—allows us to take advantage of the latent heat already contained in the rising mist to help vaporize the ethanol within the separately introduced mash mixture ... which will then move up the column with the reboiler-pro duced "steam".

When the vapors leave the stripper circuit, they flow-through the interconnecting pipe—to the rectifier column, where they increase in strength to about 170 proof after passing through the pall-ring packing. Then, in order to maintain a temperature differential between the top and bottom of the rectifier and to keep the upper portion of the packing wet (both of which are necessary to the fractionation process), an internal refluxing heat exchanger-controlled by a temperaturesensitive three—way flow valve—is used to circulate cold water through the reflux section at the top of the rectifier column.

In addition, it's at this point that the 170-proof ethanol is upgraded to 185 proof or higher. The increase in potency is brought about, in part, by the cool heat exchanger (which condenses some of the alcohol—rich vapors within the conduit), and by the introduction of high—proof alcohol from either the storage tank or a separate reservoir. Refluxing as much as 50% of the final product in this manner can increase the ethanol's strength to a maximum of 192 proof. (This supplemental feed tends to create an accumulation of fuel and water at the base of the rectifier column, so the reusable liquid is returned to the top of the stripper column by a sealless magnetically driven gear pump.)

From the rectifier, the fuel vapors go directly to the first stage (or upper section) of the condenser column, where incoming mash-circulating through coiled tubing on its way to the stripper-absorbs latent heat from the passing gases and starts their "precipitation" process. The component's second stage is composed of a Liebig (tube-within-a-tube) condenser surrounded by yet another tubing coil. Both of these simple heat exchangers eventually carry cool water to the tubing maze in the reflux section, but before doing so they condense the remainder of the alcohol vapors passing through the column, as well as any ethanol mist that may exist in the discharged—or pumped-out-air. (The vacuum draw pipe is actually the center tube of the Liebig condenser, so it's kept "droplet-forming" cold at all times.)

After the liquid alcohol leaves the condenser, it passes through a continuous proofing device (made from PVC pipe and Pyrex glass), and then into a storage tank which is, like the still, kept in a partial vacuum. (By keeping the container under negative pressure, too, we're able to eliminate a pump that would otherwise be needed to pull the ethanol from the vacuum system to an atmospheric condition.)

VACUUM ANYONE?

As we mentioned earlier, this still can be built as either a normal pressure or a vacuum-aided apparatus (if the latter feature is eliminated, however, approximately 6-1/2 times more surface area must be added to the reboiler heat exchanger). In its vacuum mode, as Goosen chose to build it, the distillery uses a watersealed and—cooled Kinney "liquid ring" air pump to draw off the device's internal atmosphere, and this air is removed from a spot close to the alcohol discharge point, through the Liebig condenser's center tube.

In the course of our experimentation, we've found a vacuum pressure of 18 to 22 inches of mercury to be about the ideal range in which to work. At the high end of this scale, the reboiler temperature needs to be only 125F, that at the top of the stripper tower 115F, and that in the uppermost section of the rectifier 95F, in order for distillation to take place. A greater vacuum increase would, of course, lower the boiling point still further, but would also have the undesirable effect of simultaneously decreasing the volume of vapors that could be carried through the columns, which in effect would reduce the capacity of a givendiameter tube by half, or more, in comparison to an equivalent pipe in a normal still ... and thus lower the distillery's production capability.

Under a high vacuum load, any negatively aspirated still will have a tendency to "vapor lock", since there isn't enough atmosphere present to lift the heavy vapors and keep them flowing. To cure this problem, we've introduced an adjustable "artificial leak" into the system, which promotes a limited vapor flow and also provides a means of controlling the depth of the vacuum draw. Furthermore, negative-atmosphere stills tend to heat up evenly throughout, thereby discouraging proper fractionation . . . but this quirk has been checked by the introduction of cool mash into the top of the stripper, as well as by the use of a heat exchanger in the reflux section of the rectifier column.

As a result of our compensating for the idiosyncrasies inherent in the vacuum system, we're able to feed the still at a rate of 48 gallons per hour, and collect about six gallons of fuel-grade alcohol over the same length of time.

A BOON TO SMALL-SCALE FUEL PRODUCERS

On the surface, it might appear that the application of vacuum principles to the distillation of alcohol would enable a fuel producer to reduce his or her still's energy requirements by an extraordinary measure. Unfortunately, the only true "economy of BTU" present in a vacuum system occurs in the saving of sensible heat, or that which is required to raise the temperature of the mash from ambient to the brink of boiling. But the additional energy that's then needed to convert the heated liquid into vapor (this is known as latent heat) is still very much a factor in both normal atmosphere and vacuum setups ... so the increase in thrift of operation in a negative-pressure setup isn't as great as you might think.

Vacuum distillation does, however, offer several distinct advantages that easily offset any frustrations surrounding its energy requirements, and these especially favor small-scale operators:

[1] Hot water alone can provide all the heat necessary for the successful distillation of alcohol. This eliminates the need for costly federal—and state—approved boilers, and opens the door to the use of inexpensive homebuilt solar collectors.

[2] The mash doesn't require much preheating, so the system is brought into equilibrium faster than it would be in a conventional still . . . thus saving time, energy, and alcohol.

[3] The distillery can operate within a broad range of temperatures, making the system quite flexible, since the vacuum pressure will adjust—automatically—to any increase or decrease of heat in the reboiler.

[4] If all the component parts are reliable, the still will come into a steady state early in the run, and remain there for the duration. This is probably our unit's single most desirable feature, since it eliminates the need for distillery supervision .. . especially if an automatic safety device is used to shut down the system should the mash or fuel supply run out.

After weighing the benefits and weaknesses of an "evacuated" distillery, we're convinced that the pressure—relieved system—even though it might be slightly more costly and tedious to build than is a conventional still—is well worth the extra effort, especially for the part—time fuel producer. And as an added bonus the design shown here can be increased in size, if necessary (see the accompanying chart), to fit a distiller's specific needs. It'd be pretty difficult to find a fuel-distilling system-either homebuilt or factory madethat answers the needs of the "little guy" (or gal) as well as this one does. And after all, that's exactly the person we designed it for!

UPSCALING SPECIFICATION
Column diameter 8"' 10" 12"
Stripper column height (minimum maximum) 10-15' 12.5-18' 15-22.5'
Rectifier column height (minimum maximum) 13-18' 16-22' 19-27'
Reboiler capacity (gallons) 50-100 100 100
Reboiler heat exchanger area (square feet) 44 70 90
Mash feed (gallons per hour) 48 75 100
Reboiler BTU input required (per hour) 74,640 116,625 155,500
Recommended mash feed pump Roper progressive-cavity type, Model 7-025
Recommended discharge pump Teel rotary-screw type, Model 1P898
Recommended vacuum pump Kinney liquid-ring type, Model KLRC-3
Recommended bottom return pump Tuthill magnet-drive gear type, Model 9239
Recommended alcohol discharge pump Micro magnet-drive gear type. Model 122 651-10A

 

 
















Henry Ford and Fuel Ethanol

Why Henry's plans were delayed for more than a half century

Ford Model PEthanol has been known as a fuel for many decades.

Indeed, when Henry Ford designed the Model T, it was his expectation that ethanol, made from renewable biological materials, would be a major automobile fuel.

However, gasoline emerged as the dominant transportation fuel in the early twentieth century, because of the ease of operation of gasoline engines with the materials then available for engine construction, and a growing supply of cheaper petroleum from oil field discoveries.

But gasoline had many disadvantages as an automotive source. The “new” fuel had a lower octane rating than ethanol, was much more toxic (particularly when blended with tetra-ethyl lead and other compounds to enhance octane), was generally more dangerous, and contained threatening air pollutants. Petroleum was more likely to explode and burn accidentally, gum would form on storage surfaces, and carbon deposits would form in combustion chambers of engines. Pipelines were needed for distribution from “area found” to “area needed”. Petroleum was much more physically and chemically diverse than ethanol, necessitating complex refining procedures to ensure the manufacture of a consistent “gasoline” product.

Because of its lower octane rating relative to ethanol, the use of gasoline meant the use of lower compression engines and larger cooling systems.

Diesel engine technology, which developed soon after the emergence of gasoline as the dominant transportation fuel, also resulted in the generation of large quantities of pollutants.

However, despite these environmental flaws, fuels made from petroleum have dominated automobile transportation for the past three-quarters of a century. There are two key reasons: First, cost per kilometre of travel has been virtually the sole selection criteria. Second, the large investments made by the oil and auto industries in physical capital, human skills and technology make the entry of a new cost-competitive industry difficult.

Until very recently, environmental concerns have been largely ignored. But all of that is finally changing as consumers demand fuels, such as ethanol, which are much kinder to the natural environment, and human health.

 
 
















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